Comments (2)
KlementineJBS
commented on June 19, 2024
IR
from usyd_phd_eln.
KlementineJBS
commented on June 19, 2024
NMR
20221108_BG_8C_2.zip
20221108_BG_8C_1.zip
20221108_BG_8C proton and carbon 500 MHz.pdf
13C NMR (126 MHz, DMSO) δ 163.18, 160.26, 152.86, 151.12, 149.88, 149.59, 141.14, 137.63, 123.03, 120.39, 109.95, 101.15, 56.12, 55.08.
1H NMR (500 MHz, DMSO-d6) δ 11.42 (s, 1H), 8.61 (d, J = 4.4 Hz, 1H), 7.98 (d, J = 7.9 Hz, 1H), 7.89 (t, J = 7.8 Hz, 1H), 7.63 (t, J = 7.9 Hz, 1H), 7.35 – 7.29 (m, 1H), 6.67 (d, J = 7.7 Hz, 1H), 6.34 (d, J = 7.9 Hz, 1H), 4.14 (s, 1H), 4.05 (s, 3H).
from usyd_phd_eln.
Related Issues (20)
- KBS50-1 - Nosyl protection of bis(3-aminopropyl)amine HOT 13
- KBS44-2 - Nosyl deprotection of KBS49 HOT 10
- KBS50-2 - Nosyl protection of bis(3-aminopropyl)amine HOT 9
- KBS53-1 - Nosyl deprotection of KBS48 HOT 12
- KBS52-1 - Nosyl deprotection of KBS51 HOT 7
- KBS51-1 - Mitsunobu reaction with KBS28 and KBS50 HOT 10
- KBS53-2 - Nosyl deprotection of KBS48 HOT 9
- KBS48 (pooled) - purification HOT 3
- KBS52-2 - Nosyl deprotection of KBS51 HOT 2
- KBS51-2 - Mitsunobu reaction with KBS28 and KBS50 HOT 5
- KBS22-2 - Linear click coupling of bis-propargyl diaminohexane and azidoadamantane HOT 6
- Carlota's compounds - for purification HOT 2
- KBS22-3 - Linear click coupling of bis-propargyl diaminohexane and azidoadamantane HOT 8
- KBS52-3 - Nosyl deprotection of KBS51 HOT 15
- 2024_BG_A_1 - Formation of benzoyl thioureas HOT 2
- 2024_BG_B_1 - Hydrolysis of benzoyl thioureas HOT 2
- SAR - for future aminothiazoles
- 2024_BG_C - characterisation of final compounds HOT 4
- 2023_BG_12C
- more samples
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