Comments (3)
KlementineJBS
commented on June 10, 2024
NMR for 4-17 looks best - still has some impurities though.
BG_8D 4-17_1.zip
BG_8D 36-46_1.zip
BG_8D 18-30_1.zip
BG_8D 31-35_1.zip
from usyd_phd_eln.
KlementineJBS
commented on June 10, 2024
Column 2
BG_8D flask_1.zip - 31.9 mg
BG_8D F1-10_1.zip - 143.5 mg
BG_8D F13-17_1.zip - 30.3 mg
BG_8D F18-22_1.zip - 14.5 mg
BG_8D fractions (2nd column).pdf
Fractions 13-17 is the most clean and will be used for testing etc.
from usyd_phd_eln.
KlementineJBS
commented on June 10, 2024
23.11.22
BG_8D 13-17 23-11-22_1.zip
BG_8D 18-22 23-11-22_1.zip
After final cleaning, 18-22 is actually cleaner.
from usyd_phd_eln.
Related Issues (20)
- KBS43-3 - Nosyl protection of 1,6-diaminohexane HOT 4
- KBS48-1 - Mitsunobu reaction with KBS28 and KBS43 HOT 7
- KBS23-8 - Azidation of 1-naphthylamine HOT 2
- KBS28-9 - Click coupling of 1-azidonaphthalene and propargyl alcohol HOT 6
- KBS49-1 - Mitsunobu reaction with KBS28 and KBS45 HOT 9
- KBS49-2 - Mitsunobu reaction with KBS28 and KBS45 HOT 17
- KBS48-2 - Mitsunobu reaction with KBS28 and KBS43 HOT 15
- KBS44, 52, 53 (Nosyl deprotection) - master page HOT 4
- KBS50-1 - Nosyl protection of bis(3-aminopropyl)amine HOT 13
- KBS44-2 - Nosyl deprotection of KBS49 HOT 10
- KBS50-2 - Nosyl protection of bis(3-aminopropyl)amine HOT 9
- KBS53-1 - Nosyl deprotection of KBS48 HOT 12
- KBS52-1 - Nosyl deprotection of KBS51 HOT 7
- KBS51-1 - Mitsunobu reaction with KBS28 and KBS50 HOT 10
- KBS53-2 - Nosyl deprotection of KBS48 HOT 9
- KBS48 (pooled) - purification HOT 3
- KBS52-2 - Nosyl deprotection of KBS51 HOT 2
- KBS51-2 - Mitsunobu reaction with KBS28 and KBS50 HOT 5
- KBS22-2 - Linear click coupling of bis-propargyl diaminohexane and azidoadamantane HOT 6
- Carlota's compounds - for purification HOT 2
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