Comments (3)
KlementineJBS
commented on June 9, 2024
H NMR
Can combine F1 and F2-3.
BG_8E F2-3_1.zip
BG_8E F1_1.zip
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KlementineJBS
commented on June 9, 2024
IR
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KlementineJBS
commented on June 9, 2024
NMR
20221108_BG_8E_1.zip
20221108_BG_8E_2.zip
20221108_BG_8E proton and carbon 500 MHz.pdf
13C NMR (126 MHz, DMSO) δ 159.84, 152.75, 152.37, 149.92, 149.54, 147.57, 141.38, 137.67, 123.10, 120.37, 115.70, 110.73, 109.83.
1H NMR (500 MHz, DMSO-d6) δ 11.75 (s, 1H), 8.61 (s, 1H), 7.98 (d, J = 7.8 Hz, 1H), 7.89 (t, J = 7.6 Hz, 1H), 7.80 – 7.73 (m, 2H), 7.36 – 7.29 (m, 1H), 7.12 (d, J = 8.2 Hz, 1H), 7.04 (d, J = 7.6 Hz, 1H).
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Related Issues (20)
- KBS48-2 - Mitsunobu reaction with KBS28 and KBS43 HOT 15
- KBS44, 52, 53 (Nosyl deprotection) - master page HOT 4
- KBS50-1 - Nosyl protection of bis(3-aminopropyl)amine HOT 13
- KBS44-2 - Nosyl deprotection of KBS49 HOT 10
- KBS50-2 - Nosyl protection of bis(3-aminopropyl)amine HOT 9
- KBS53-1 - Nosyl deprotection of KBS48 HOT 12
- KBS52-1 - Nosyl deprotection of KBS51 HOT 7
- KBS51-1 - Mitsunobu reaction with KBS28 and KBS50 HOT 10
- KBS53-2 - Nosyl deprotection of KBS48 HOT 9
- KBS48 (pooled) - purification HOT 3
- KBS52-2 - Nosyl deprotection of KBS51 HOT 2
- KBS51-2 - Mitsunobu reaction with KBS28 and KBS50 HOT 5
- KBS22-2 - Linear click coupling of bis-propargyl diaminohexane and azidoadamantane HOT 6
- Carlota's compounds - for purification HOT 2
- KBS22-3 - Linear click coupling of bis-propargyl diaminohexane and azidoadamantane HOT 8
- KBS52-3 - Nosyl deprotection of KBS51 HOT 15
- 2024_BG_A_1 - Formation of benzoyl thioureas HOT 2
- 2024_BG_B_1 - Hydrolysis of benzoyl thioureas HOT 2
- SAR - for future aminothiazoles
- 2024_BG_C - characterisation of final compounds HOT 3
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